Question
Describe the electrolytic refining method for the purification of metals.

Answer

  • The metals obtained from their ores are not very pure.
  • Hence, it is essential to purify the metals.
  • The most widely used method for refining impure metals is electrolytic refining.
  • [Electrolytic refining of copper]
  • Metals such as copper, zinc, tin, nickel, silver and gold are refined by electrolytic process.
  • In this process, the impure metal is made the anode and a thin strip of pure metal is made the cathode.
  • A solution of the metal salt is used as an electrolyte.
  • The apparatus is set up as shown in the figure
  • On passing the electric current through the electrolyte, the pure metal from the anode dissolves into electrolyte.
  • An equivalent amount of pure metal from the electrolyte is deposited on the cathode.
  • For example,
  • At anode (+): $Cu ( s ) \rightarrow Cu ^{2+}( aq )+2 e ^{-}$ (Impure)
  • At cathode (-): $Cu ^{2+}( aq )+2 e ^{-} \rightarrow Cu ( s )$ (Pure)
  • Net reaction: $Cu ( s ) \rightarrow Cu ( s )$ (Impure) (Pure)
  • The soluble impurities pass into the solution while the insoluble impurities such as gold, silver, platinum are settled at the bottom of the anode and are called anode-mud.

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